HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiosemicarbazide → HCID 3002293, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiosemicarbazide | HCID 2723789 | — |
| Reactant | N-(3-Fluoro-4-formylphenyl)acetamide | HCID 10214430 | — |
| Product | HCID 3002293 | HCID 3002293 | 45% |
Reaction Steps
4-Acetamido-2-fluorobenzaldehyde 20 then is reacted with thiosemicarbazide to form 4-acetamido-2-fluorobenzaldehyde thiosemicarbazone 17 in 45% yield. An exemplary scheme for this reaction is shown below.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06624153B2 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-6b97c32cc8cc44d99c59889631ae12ff |
| Source note | uspto-grants-2003_09 |