HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Furancarbonyl chloride → HCID 22992449, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Furancarbonyl chloride | HCID 68242 | — |
| Reactant | Methyl 4-(4-aminophenyl)-4-oxobutanoate | HCID 12016833 | — |
| Product | HCID 22992449 | HCID 22992449 | 46% |
Reaction Steps
In a manner similar to that described in Example 3, furoyl chloride (0.044 g, 0.00034 mol) was allowed to react with 4-(4-amino-phenyl)-4-oxo-butyric acid, methyl ester (0.052 g, 0.00025 mol), and the resulting intermediate was hydrolyzed to give 0.033 g of 4-[4-(2-furoylamino)-phenyl]-4-oxo-butyric acid as an off-white solid; MS-(AP+) MH+288.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06624196B2 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-2305892d75464af68c1560993a621ae2 |
| Source note | uspto-grants-2003_09 |