HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1168520Generated: October 31, 2026
Diethyl (ethoxymethylene)malonate → HCID 12083046, compound
https://huagongshe.com/reaction/1168520
Participants
| Role | Name | HCID | Charge |
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| Reactant | Diethyl (ethoxymethylene)malonate | HCID 6871 | — |
| Reactant | 2-Amino-5-methylbenzyl alcohol | HCID 576450 | — |
| Product | HCID 12083046 | HCID 12083046 | 87% |
Reaction Steps
A mixture of 2-(hydroxymethyl)-4-methylaniline (10.0 g) and diethyl ethoxymethylenemalonate (18.5 g) is heated at 110° C. for 1 h. Crystallization from ether/hexane afforded 19.5 g of the title compound. Physical characteristics: M.p. 92-95° C.; Anal. Found: C, 62.49; H, 6.88; N, 4.60.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06624159B2 |
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| Source dataset | uspto-grants-2003_09 |
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| ORD ID | ord-040439b35660435588d4dd8df742cb80 |
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| Source note | uspto-grants-2003_09 |
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