HuagongsheHuagongshe Chemistry Print Report · For research reference only
(Phenylmethoxy)acetaldehyde → 2-(Benzyloxy) ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (Phenylmethoxy)acetaldehyde | HCID 108989 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Product | 2-(Benzyloxy) ethanol | HCID 12141 | — |
| Product | (Phenylmethoxy)acetaldehyde | HCID 108989 | — |
Reaction Steps
Example 1 was repeated except that 2.5 g (30 mmoles) of sodium hydrogen carbonate was used instead of 2.6 g (15 mmoles ) of dipotassium hydrogen phosphate, to obtain 7.1 g of benzyloxyacetaldehyde and 4.5 g of 2-benzyloxyethanol (yield of benzyloxyacetaldehyde based on the 2-benzyloxyethanol that had reacted: 66.8%, ratio of recovery of 2-benzyloxyethanol: 29.6%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06624331B1 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-016bf7d79d9742119113d1bb520a0dce |
| Source note | uspto-grants-2003_09 |