HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 102262612, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 102262609 | HCID 102262609 | — |
| Product | HCID 102262612 | HCID 102262612 | — |
Reaction Steps
Into ethyl acetate was dissolved IM-8 (42 g) which was obtained as described above. NaI (42.5 g) was added. This mixture was refluxed for three hours. The reaction mixture was concentrated, and then refined with silica gel column chromatography (ethyl acetate/hexane) to obtain 36.3 g of IM-9.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06627099B2 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-f1eb679a175c4a4595044e2ce17bcf31 |
| Source note | uspto-grants-2003_09 |