HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10122634, compound → HCID 10283374, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10122634 | HCID 10122634 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 10283374 | HCID 10283374 | — |
Reaction Steps
A mixture of Example 39 (34.0 mg, 0.050 mmol) and 10% Pd/C (5.0 mg) in ethanol (2.0 mL) at room temperature was stirred under hydrogen for 16 hours, filtered through diatomaceous earth (Celite®) with ethanol rinsing, and concentrated to provide the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06627767B2 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-38c49f9be7494d51a5ede70670b8290d |
| Source note | uspto-grants-2003_09 |