Methylamine → HCID 58985728, compound

HRID 1169736Notes

Reaction equation

HRID 1169736 reaction equation
[Cl:1][C:2]1[N:7]=[C:6](Cl)[C:5](I)=[CH:4][N:3]=1.[CH3:10][NH2:11].CC1(C)C(C)(C)OB([C:20]2[S:21][CH:22]=[CH:23][CH:24]=2)O1>>[Cl:1][C:2]1[N:7]=[C:6]([NH:11][CH3:10])[C:5]([C:20]2[S:21][CH:22]=[CH:23][CH:24]=2)=[CH:4][N:3]=1

Participants

4

Reactant 3

HCID 6329MethylamineHCID 2634382,4-Dichloro-5-iodopyrimidineHCID 107036284,4,5,5-Tetramethyl-2-(thiophen-2-yl)-1,3,2-dioxaborolane

Product 1

HCID 58985728HCID 58985728, compound

Procedure

Preparation according to procedures 2 and 3 with the use of 2,4-dichloro-5-iodopyrimidine, methylamine and 4,4,5,5-tetramethyl-2-(2-thienyl)-1,3,2-dioxaborolane.

Workup

  1. customPreparation

Sources & evidence

ORD record
ord-f204e5b36b62492299623476294c94b7
Source dataset
uspto-grants-2010_11
Patent number
US07825128B2

Reaction notes

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