HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Iodoaniline → HCID 178520827, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Iodoaniline | HCID 10893 | — |
| Reactant | 2-[(Dimethylamino)methylidene]-1,3-diphenylpropane-1,3-dione | HCID 13070769 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178520827 | HCID 178520827 | — |
Reaction Steps
A solution of 1,3-diphenyl-2-[(dimethylamino)methylene]-1,3-propanedione (317 mg, 1.13 mmol) in 5.5 mL of MeOH was treated with solid 4-iodoaniline (245 mg, 1.12 mmol). The resulting solution was stirred at rt overnight. The resulting precipitate was isolated by filtration and washed with MeOH. The title compound was isolated as a light yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07825278B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-df7fccef41e9499fa9b63c9a838da4be |
| Source note | uspto-grants-2010_11 |