HRID1170582

反应详情

EQUATION

反应方程式

HRID 1170582 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a solution of 4-methoxybenzyl 2-(N-CBZ-L-valyloxy)-propionate (7.8 g, 17.5 mmole) in dichloromethane (100 ml) was added trifluoroacetic acid (10 ml) and the solution was stirred for one hour at room temperature. The solution was evaporated under reduced pressure and the product was isolated by silica gel column chromatography. Yield: 5.0 g

WORKUP

后处理

  1. customThe solution was evaporated under reduced pressure
  2. customthe product was isolated by silica gel column chromatography