HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalic acid dihydrate → 4,5,6,7-tetrahydro-4-(2-(morpholin-4-yl)ethyl)-1-phenyl-1H-indazole oxalate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalic acid dihydrate | HCID 61373 | — |
| Reactant | 4,5,6,7-tetrahydro-4-(2-(morpholin-4-yl)ethyl)-1-phenyl-1H-indazole | HCID 11531451 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 4,5,6,7-tetrahydro-4-(2-(morpholin-4-yl)ethyl)-1-phenyl-1H-indazole oxalate | HCID 11531450 | 65% |
Reaction Steps
HO2CCO2H.2H2O (156 mg, 1.23 mmol) is added to a solution of 4,5,6,7-tetrahydro-4-(2-(morpholin-4-yl)ethyl)-1-phenyl-1H-indazole (380 mg, 1.22 mmol) in 4 mL of acetone giving 4,5,6,7-tetrahydro-4-(2-(morpholin-4-yl)ethyl)-1-phenyl-1H-indazole oxalate (318 mg, 0.79 mmol, 65%, white solid).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07829559B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-da96b50949ab40a1b732a5ab3f1c5a26 |
| Source note | uspto-grants-2010_11 |