HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59553878, compound → HCID 135948973, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59553878 | HCID 59553878 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 135948973 | HCID 135948973 | — |
Reaction Steps
2-(2-Benzyloxy-phenyl)-5-methoxy-3-phenethyl-3H-pyrido[4,3-d]pyrimidin-4-one dissolved in methanol (0.05M) was subjected to H-cube hydrogenation (room temperature, Pd/C cartridge). Solvent was then removed and product purified on preparative TLC plate to afford the desired 2-(2-Hydroxy-phenyl)-5-methoxy-3-phenethyl-3H-pyrido[4,3-d]pyrimidin-4-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07829572B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-0f22f4f12fce4152bb1da75e2880dce7 |
| Source note | uspto-grants-2010_11 |