HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2,3-Benzothiadiazole-5-carboxylic acid → HCID 59553346, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2,3-Benzothiadiazole-5-carboxylic acid | HCID 2735458 | — |
| Reactant | 4-(2-Morpholinoethoxy)naphthalen-1-amine | HCID 11043912 | — |
| Product | HCID 59553346 | HCID 59553346 | — |
Reaction Steps
Compound is prepared from benzo[1,2,3]thiadiazole-5-carboxylic acid and 4-(2-morpholin-4-yl-ethoxy)-naphthalen-1-ylamine according to conditions described in general procedure G. Mp: 188-190° C.; 1H NMR (300 MHz, CDCl3) δ 2.70 (t, 4H), 3.00 (t, 2H), 3.78 (t, 4H), 4.30 (t, 2H), 6.82 (d, 1H), 7.58 (m, 2H), 7.65 (d, 1H), 7.88 (d, 1H), 8.15 (d, 1H), 8.25 (d, 2H), 8.40 (s, 1H), 9.18 (s, 1H); MS 435 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07829560B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-b333ae482c6b422a971845289e45f200 |
| Source note | uspto-grants-2010_11 |