反应详情

The procedure is the same as that described above, using 14 g of methyl 2-benzyloxy-4-iodobenzoate, 350 ml of toluene and 72 ml of DiBAlH. The product is purified by chromatography on a silica column, eluted with a heptane/ethyl acetate 9:1 mixture. After evaporation of the solvents, 12.2 g (99%) of the expected compound are recovered in the form of a yellow oil.

1. customThe product is purified by chromatography on a silica column
2. washeluted with a heptane/ethyl acetate 9:1 mixture
3. customAfter evaporation of the solvents, 12.2 g (99%) of the expected compound
4. customare recovered in the form of a yellow oil