HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 86054527, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 68767917 | HCID 68767917 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 86054527 | HCID 86054527 | — |
Reaction Steps
The procedure is the same as that described above, using 6.6 g, that is 18.8 mmol, of (4-iodo-2-phenethyloxyphenyl)methanol, 1.8 ml of oxalyl chloride and 3 ml of DMSO. After evaporation of the solvents, 6.4 g (96%) of the expected compound are recovered in the form of a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07829588B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-764bdffd3f2c4c83ba26638ec00df4d7 |
| Source note | uspto-grants-2010_11 |