HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 23138766, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 23139066 | HCID 23139066 | — |
| Product | HCID 23138766 | HCID 23138766 | 68% |
Reaction Steps
Following a procedure similar to that described in Example 150-(d), (E)-3-{[1-(methoxycarbonylmethyl)-1H-tetrazol-5-yl]methylidene}-1-(triphenylmethyl)piperidin-4-one (Example 150-(c), 2.2 g) was reduced with sodium borohydride. Purification gave the title compound (1.5 g, yield: 68%) as a pale yellow amorphous solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07829580B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-9ed2529be2ea479bb11b94d506c217c1 |
| Source note | uspto-grants-2010_11 |