Sodium Hydroxide → HCID 57995680, compound

Participants

Reaction Steps

In step (2), 1-chloropropanol-3,3-dinitroazetidine of Formula IV prepared in step (1) is cooled, and NaOH aqueous solution is slowly dropped. Thus obtained brown solution is warmed to room temperature and stirred for 3-10 hours. The solution obtained is washed with distilled water and then distilled with diethylether. Thus obtained organic layer is dried on K2CO3. The solvent is removed under lowered pressure and 1-glycidyl-3,3-dinitroazetidine is obtained.

Provenance & Evidence