HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 68772395, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 68771954 | HCID 68771954 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 68772395 | HCID 68772395 | — |
Reaction Steps
A solution of Example 58A (650 mg, 1.07 mmol) in 3 mL each of CH2Cl2 and methanol was treated with hydrazine hydrate (336 μL). Ethyl acetate and 1N NaOH were added. The organic phase was dried (Na2SO4) and concentrated in vacuo to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07834012B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-8b46b2ac29414460a416040d52182f63 |
| Source note | uspto-grants-2010_11 |