HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Benzoylpiperazine hydrochloride → HCID 57562609, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Benzoylpiperazine hydrochloride | HCID 12203351 | — |
| Reactant | HCID 57562669 | HCID 57562669 | — |
| Product | HCID 57562609 | HCID 57562609 | — |
Reaction Steps
The amination reaction was performed in the same manner as in Example 16-(3) using 6-(methanesulfonyloxymethyl)-5-(((tert-butyl(dimethyl)silyl)oxy)methyl)-N-(1,2,4-thiadiazol-5-yl)pyridin-2-amine and 1-benzoylpiperazine hydrochloride obtained in the same manner as in Reference Example 1. Then, the deprotection reaction was performed in the same manner as in Example 5-(3) to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07834018B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-9ff7d94d79ef45a591190e586e473283 |
| Source note | uspto-grants-2010_11 |