HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluoro-3-methylbenzenepropanol → HCID 57659624, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluoro-3-methylbenzenepropanol | HCID 57659610 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 57659624 | HCID 57659624 | 60.2% |
Reaction Steps
According to procedures described above, 3-(2-fluoro-3-methyl-phenyl)-propan-1-ol (300 mg, 1.78 mmol) was oxidized by PCC in DCM to give 178 mg (60%) of 3-(2-fluoro-3-methyl-phenyl)-propionaldehyde. LC-MS: tR=0.86 min; [M+H]+=no ionization.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07834028B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-7efa0f6ded074a87a60a96d61ddc5b35 |
| Source note | uspto-grants-2010_11 |