HRID1172681

反应详情

EQUATION

反应方程式

HRID 1172681 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

800 mg 4-Fluoro-2-vinyl-benzonitrile were dissolved in 5 ml methanol. 80 mg palladium (10% on charcoal) were added and the reaction was stirred under a hydrogen atmosphere for one hour. The catalyst was filtered off trough a pad of celite. The filtrate was evaporated to obtain 625 mg 2-Ethyl-4-fluoro-benzonitrile.

WORKUP

后处理

  1. filtrationThe catalyst was filtered off trough a pad of celite
  2. customThe filtrate was evaporated