HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosuccinimide → HCID 68689537, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | HCID 68688070 | HCID 68688070 | — |
| Reactant | HCID 68692013 | HCID 68692013 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 68689537 | HCID 68689537 | — |
Reaction Steps
A mixture of Example 4, D6 (1 eq) and N-chlorosuccinimide (2 eq) in THF was stirred at RT. The solvent was removed under reduced pressure and the resulting crude was used as such in the next step without purification. MS (ES) C16H12ClFN2O3 requires: 334, found: 335 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07834015B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-fbbb5a1d62694ae18fe0d3ca31d8f3e2 |
| Source note | uspto-grants-2010_11 |