HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12767831, compound → 2-Propyl-4-(4-chlorophenoxy)phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12767831 | HCID 12767831 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 2-Propyl-4-(4-chlorophenoxy)phenol | HCID 18772262 | 99.6% |
Reaction Steps
A mixture of the product from step 4 (15.7 g, 60 mmol) and 10% Pd/C (3.1 g) in ethyl acetate (300 mL) was stirred under hydrogen (1 atm). After the reaction was completed (ca. 30 min), the mixture was filtered through celite and the filtrate was concentrated to give 15.7 g of the title compound as an oil which solidified upon standing.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07834036B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-e571cbcda72748c38d02b2a2e1494a82 |
| Source note | uspto-grants-2010_11 |