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HRID1172993

反应详情

EQUATION

反应方程式

HRID 1172993 的结构方程式

REACTANTS

反应物

3
结构：O=Cc1ncc[nH]1
HCID24955

1H-Imidazole-2-carboxaldehyde

C4H4N2O

结构：CC1COc2ccccc2N1
HCID2763760

3-Methyl-3,4-dihydro-2H-1,4-benzoxazine

C9H11NO

结构：[BH3-]C#N.[Na+]
HCID5003444

Sodium cyanotrihydroborate

CH3BNNa

PRODUCTS

生成物

1
结构：CC1COc2ccccc2N1Cc1ncc[nH]1
HCID59556803

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Cl-].[Cl-].[Zn+2]
催化剂HCID3007855

Zinc chloride

Cl2Zn

结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

Prepared analogously to Example 1, from (RS)-3-methyl-3,4-dihydro-2H-benzo[1,4]oxazine, imidazole-2-carboxaldehyde, zinc chloride and sodium cyanoborohydride in methanol. MS (ISP): 230.4 ([M+H]+).