Hydrochloric Acid → HCID 22674054, compound

Participants

Reaction Steps

N-Boc-1-methyl-2-(3-ethoxycarbonylaminophenyl)ethylamine (1.173 g, crude) was dissolved in ethanol (5.0 ml), to which was then added hydrochloric acid (5 ml), followed by stirring at room temperature for 1.5 hours. Then, hydrochloric acid (2.5 ml) was further added thereto, followed by stirring at room temperature for 2 hours. The solvent was evaporated, to give the title compound (1.148 g, crude) as a yellow oil. It was used in the next reaction without carrying out a further purification.

Provenance & Evidence