HRID1173337

反应详情

EQUATION

反应方程式

HRID 1173337 的结构方程式

PROCEDURE

实验过程

The product from Step A (0.227 g) was treated with 0.070 g (0.71 mmol) of cyclohexanone according to the procedure described in Example 3. The product was purified on a silica gel flash chromatography column eluted with 5-10% isopropanol in hexane. Evaporation of the purified fractions and drying in vacuo afforded the title compound.

WORKUP

后处理

  1. customThe product was purified on a silica gel flash chromatography column
  2. washeluted with 5-10% isopropanol in hexane
  3. customEvaporation of the purified fractions
  4. customdrying in vacuo