HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanone → {2-[2-(Benzyloxy)-4,6-di-tert-butylphenyl]ethyl}cyclohexylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanone | HCID 7967 | — |
| Reactant | {2-[2-(Benzyloxy)-4,6-di-tert-butylphenyl]ethyl}amine | HCID 68714462 | — |
| Product | {2-[2-(Benzyloxy)-4,6-di-tert-butylphenyl]ethyl}cyclohexylamine | HCID 68717844 | — |
Reaction Steps
The product from Step A (0.227 g) was treated with 0.070 g (0.71 mmol) of cyclohexanone according to the procedure described in Example 3. The product was purified on a silica gel flash chromatography column eluted with 5-10% isopropanol in hexane. Evaporation of the purified fractions and drying in vacuo afforded the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07834062B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-4dfe015a8991481bb312a1f3373c367d |
| Source note | uspto-grants-2010_11 |