HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxyphenol → HCID 11633101, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxyphenol | HCID 9015 | — |
| Reactant | 4-[(2-Hydroxyethyl)(2,2,2-trifluoroethyl)amino]-2-(trifluoromethyl)benzonitrile | HCID 86623731 | — |
| Product | HCID 11633101 | HCID 11633101 | — |
Reaction Steps
Synthesized as described in Example 1C using 4-[(2-hydroxyethyl)(2,2,2-trifluoroethyl)amino]-2-(trifluoromethyl)benzonitrile and 4-methoxyphenol: 1H NMR (300 MHz, CD3OD) δ 7.73 (d, J=9.0 Hz, 1H), 7.36 (d, J=2.3 Hz, 1H), 7.25 (dd, J=9.0 Hz, 2.5 Hz, 1H), 6.80 (app. s, 4H), 4.42 (q, J=8.9 Hz, 2H), 4.17 (t, J=5.1 Hz, 2H), 4.00 (t, J=5.1 Hz, 2H), 3.51 (s, 3H); MS (APCI) m/z 419 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07834063B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-9d6faabe70c14f6897f54d216a2a57f0 |
| Source note | uspto-grants-2010_11 |