4-Hydroxy-2-methylbenzaldehyde → HCID 86623734, compound

Participants

Reaction Steps

Synthesized as described in Example 1C from 4-[(2-hydroxyethyl)(2,2,2-trifluoroethyl)amino]-2-(trifluoromethyl)benzonitrile and methyl 4-hydroxybenzaldehyde: 1H NMR (300 MHz, CDC3) δ 9.89 (s, 1H), 7.88-7.80 (m, 2H), 7.68 (d, J=8.9 Hz, 1H), 7.20 (d, J=2.4 Hz, 1H), 7.02 (dd, J=8.8, 2.7 Hz, 1H, partially overlapped with 6.99-6.93), 6.99-6.93 (m, 2H), 4.31 (t, J=5.2 Hz, 2H), 4.20 (q, J=8.5 Hz, 2H), 4.05 (t, J=5.2 Hz, 2H).

Provenance & Evidence