4'-Bromoacetanilide → HCID 11591004, compound

HRID 1173487Notes

Reaction equation

HRID 1173487 reaction equation
[C:1]([C:3]1[CH:8]=[CH:7][C:6]([N:9]([CH2:18][CH:19]=[CH2:20])[CH2:10][C:11]([O:13][C:14]([CH3:17])([CH3:16])[CH3:15])=[O:12])=[CH:5][C:4]=1[C:21]([F:24])([F:23])[F:22])#[N:2].[CH3:25][C:26]([NH:28][C:29]1[CH:34]=[CH:33][C:32](Br)=[CH:31][CH:30]=1)=[O:27]>>[C:26]([NH:28][C:29]1[CH:34]=[CH:33][C:32]([CH2:20][CH2:19][CH2:18][N:9]([C:6]2[CH:7]=[CH:8][C:3]([C:1]#[N:2])=[C:4]([C:21]([F:23])([F:22])[F:24])[CH:5]=2)[CH2:10][C:11]([O:13][C:14]([CH3:16])([CH3:17])[CH3:15])=[O:12])=[CH:31][CH:30]=1)(=[O:27])[CH3:25]

Participants

3

Reactant 2

HCID 76834'-BromoacetanilideHCID 11186852HCID 11186852, compound

Product 1

HCID 11591004HCID 11591004, compound

Procedure

Synthesized according to Example 84B from 1,1-dimethylethyl N-[4-cyano-3-(trifluoromethyl)phenyl]-N-2-propen-1-ylglycinate and 4-bromoacetanilide: MS (APCI) m/z 498 ([M+Na]+), 420 ({[M+H]—C4H8}+).

Workup

  1. customSynthesized

Sources & evidence

ORD record
ord-596308ff48bc4c9ebb32ce18d9ec5a87
Source dataset
uspto-grants-2010_11
Patent number
US07834063B2

Reaction notes

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