HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 68635447, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 56557142 | HCID 56557142 | — |
| Product | HCID 68635447 | HCID 68635447 | — |
Reaction Steps
Synthesized as described in Example 70B from 4-[(2-{[4-(methyloxy)phenyl]oxy}ethyl)amino]-2-(trifluoromethyl)benzonitrile, excluding TFA deprotection of tert-butyl ester. Purified by flash chromatography (EtOAc/hexanes), obtained as a colorless gum: MS (APCI) m/z 451 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07834063B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-c38afce03ca14654a6fe0e45207f885a |
| Source note | uspto-grants-2010_11 |