HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59556894, compound → HCID 67105492, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59556894 | HCID 59556894 | — |
| Reactant | L-SELECTRIDE tetrahydrofuran | HCID 131725857 | — |
| Product | HCID 67105492 | HCID 67105492 | — |
Reaction Steps
Using 2-chloro-4-(3,3-diethyl-5-methyl-2,4-dioxopyrrolidin-1-yl)benzonitrile (67 mg) and lithium tri(sec-butyl)borohydride-THF solution (0.33 mL, 1 mol/L), and in the same manner as in Example 5, the title compound was obtained as colorless crystals (yield: 34.5 mg, 51%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07834051B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-ac6f388063f646b5a30cda207e0c5917 |
| Source note | uspto-grants-2010_11 |