HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86639466, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 59203392 | HCID 59203392 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86639466 | HCID 86639466 | 50% |
Reaction Steps
Methyl (4S,5S)-2-methyl-4-propyl-4,5-dihydro-1,3-oxazole-5-carboxylate (0.2 g, 1.1 mmol), methanol (2 ml) and concentrated hydrochloric acid (0.25 ml) were mixed, and the mixture was stirred at room temperature for 3 hours. The solvent was evaporated away under reduced pressure to obtain the title compound as a white solid (0.1 g, yield: 50%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07834190B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-79ca3ea1ea30488dac44a95fe94974b7 |
| Source note | uspto-grants-2010_11 |