HRID1174145

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6422

未命名化合物

结构：CC[C@H](C)[C@@H](C(=O)OC(C)(C)C)N1CCN(Cc2csc(C)n2)C1=O

HCID67410059

未命名化合物

PRODUCTS

生成物

HCID6422

未命名化合物

结构：CC[C@H](C)[C@@H](C(=O)O)N1CCN(Cc2csc(C)n2)C1=O

HCID67407644

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6344

Dichloromethane

CH2Cl2

CONDITIONS

反应条件

温度: 25 °C

PROCEDURE

实验过程

A solution containing the product from Example 11C (2.0 g, 5.4 mmol) in dichloromethane (14 mL) was treated with trifluoracetic acid (7 mL), stirred at 25° C. for 3 hours and concentrated to give the title compound as a trifluoroacetic acid salt.

WORKUP

后处理

concentrationconcentrated