HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 42626244, compound → HCID 42625376, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 42626244 | HCID 42626244 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 42625376 | HCID 42625376 | — |
Reaction Steps
A solution containing the product from Example 117B (0.038 g, 0.098 mmol) in methanol (1 mL) was treated with 10% Pd on carbon (0.005 g) and the reaction was stirred under an atmosphere of hydrogen (balloon pressure) for 2 hours. The reaction was filtered and the solvent was concentrated to give the title compound, which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07834043B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-cb4f92e22ad54f61b2995467a3fc7249 |
| Source note | uspto-grants-2010_11 |