Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | HCID 86599580 | HCID 86599580 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 67407508 | HCID 67407508 | — |
Reaction Steps
A solution containing the product from Example 134A (0.122 g, 0.147 mmol) in DMF (6 mL) was treated with diethylamine (1.5 mL), stirred at 25° C. for 1 hour, and partitioned between ethyl acetate and water. The organic phase was washed with brine and dried over MgSO4, filtered and concentrated to give the title compounds.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07834043B2 |
|---|
| Source dataset | uspto-grants-2010_11 |
|---|
| ORD ID | ord-7712a878da9246fd9759d7d037c3b729 |
|---|
| Source note | uspto-grants-2010_11 |
|---|