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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1174343Generated: November 1, 2026

Diethylamine → HCID 67407508, compound

https://huagongshe.com/reaction/1174343

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiethylamineHCID 8021—
ReactantHCID 86599580HCID 86599580—
SolventDimethylformamideHCID 6228—
ProductHCID 67407508HCID 67407508—

Reaction Conditions

Temperature25 °C

Reaction Steps

A solution containing the product from Example 134A (0.122 g, 0.147 mmol) in DMF (6 mL) was treated with diethylamine (1.5 mL), stirred at 25° C. for 1 hour, and partitioned between ethyl acetate and water. The organic phase was washed with brine and dried over MgSO4, filtered and concentrated to give the title compounds.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07834043B2
Source datasetuspto-grants-2010_11
ORD IDord-7712a878da9246fd9759d7d037c3b729
Source noteuspto-grants-2010_11