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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1174359Generated: November 1, 2026

Trifluoroacetic acid → HCID 67407515, compound

https://huagongshe.com/reaction/1174359

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 67406816HCID 67406816—
SolventDichloromethaneHCID 6344—
ProductHCID 67407515HCID 67407515—

Reaction Steps

A solution of Example 145B (0.127 g, 0.35 mmol) in dichloromethane (1.75 mL) was treated with trifluoroacetic acid (1.75 mL) at 25° C. for 16 h. The solvents were evaporated, and the crude residue was azeotroped twice with ethyl acetate to give crude material which was used directly in the next step.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07834043B2
Source datasetuspto-grants-2010_11
ORD IDord-61ec6278cc8740d7b92afaff37dbd106
Source noteuspto-grants-2010_11