Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 67405859 | HCID 67405859 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 67409048 | HCID 67409048 | — |
Reaction Steps
To a solution containing the product from Example 161A (0.49 g, 1.91 mmol) in tetrahydrofuran (10.0 mL) was added aqueous HCl solution (5.0 mL, 4 N), and the mixture was stirred at 60° C. for 12 hours. The solvent was evaporated to give a white solid, which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07834043B2 |
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| Source dataset | uspto-grants-2010_11 |
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| ORD ID | ord-c5e5764b9c454f9ebcee80c5db1c4389 |
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| Source note | uspto-grants-2010_11 |
|---|