Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1174398Generated: November 1, 2026

Lithium Hydroxide → HCID 67406559, compound

https://huagongshe.com/reaction/1174398

Reaction equation

Participants

RoleNameHCIDCharge
ReactantLithium HydroxideHCID 3939—
ReactantHCID 67408147HCID 67408147—
SolventWaterHCID 962—
SolventEthyl AcetateHCID 8857—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 67406559HCID 67406559—

Reaction Steps

A solution of the product of Example 174F (0.020 g, 0.025 mmol) in a mixture of dioxane (0.250 mL) and water (0.100 mL) was added an aqueous solution of lithium hydroxide (0.028 mL, 1 N), and the mixture was stirred at room temperature for 1 hour. The reaction was diluted with ethyl acetate and washed with brine, dried over MgSO4, filtered and concentrated to give the title compound, which was used without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07834043B2
Source datasetuspto-grants-2010_11
ORD IDord-9088f03e15004973a6ccf9b789f36471
Source noteuspto-grants-2010_11