HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Methacrylate → Retinol Palmitate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Methacrylate | HCID 6658 | — |
| Reactant | Retinol | HCID 445354 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | Retinol Palmitate | HCID 5280531 | — |
Reaction Steps
An aqueous phase was prepared by dissolving 0.5 g of poly (vinyl alcohol) in 50 ml water saturated by 6 ml of ethyl acetate. An organic phase was prepared by dissolving 0.075 g Retinol Palmitate, 0.1 g mineral oil, 0.01 g of an antioxidant (chosen from BHA, BHT, tocopherol or their mixture) and 0.815 g PMMA in 5 ml of ethyl acetate. The organic phase was poured into the aqueous phase while stirring and then 100 ml of fresh water were added. The microcapsules formed were filtered, washed by water and dried at the temperature no higher 20° C. An average diameter of the microcapsules was 40 μm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07838037B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-44664d50bbee4cd3992b24b085a78fc8 |
| Source note | uspto-grants-2010_11 |