Hydrochloric Acid → HCID 86617117, compound

Participants

Reaction Steps

Methanesulfonyl chloride (30.4 mL) was added to a solution of hexane-1,3,4,6-tetraol (8.3 g) in pyridine (150 mol) at −45° C. After a reaction time at ice-bath temperature of three hours, the mixture was poured into hydrochloric acid (4 N). The resulting precipitate was filtered off with suction. The product with a molecular weight of 462.54 (C10H22O12S4) was obtained in this way; MS (ESI): 463 (M+H+).

Provenance & Evidence