Hydrochloric Acid → HCID 86617117, compound

HRID 1174572Notes

Reaction equation

HRID 1174572 reaction equation
[CH3:1][S:2](Cl)(=[O:4])=[O:3].[CH2:6]([OH:15])[CH2:7][CH:8]([OH:14])[CH:9]([OH:13])[CH2:10][CH2:11][OH:12].N1C=CC=CC=1.Cl>>[CH3:1][S:2]([O:15][CH2:6][CH2:7][CH:8]([O:14][S:2]([CH3:1])(=[O:4])=[O:3])[CH:9]([O:13][S:2]([CH3:1])(=[O:4])=[O:3])[CH2:10][CH2:11][O:12][S:2]([CH3:1])(=[O:4])=[O:3])(=[O:4])=[O:3]

Participants

5

Reactant 4

HCID 313Hydrochloric AcidHCID 1049PyridineHCID 31297Methanesulfonyl chlorideHCID 18534276HCID 18534276, compound

Product 1

HCID 86617117HCID 86617117, compound

Procedure

Methanesulfonyl chloride (30.4 mL) was added to a solution of hexane-1,3,4,6-tetraol (8.3 g) in pyridine (150 mol) at −45° C. After a reaction time at ice-bath temperature of three hours, the mixture was poured into hydrochloric acid (4 N). The resulting precipitate was filtered off with suction. The product with a molecular weight of 462.54 (C10H22O12S4) was obtained in this way; MS (ESI): 463 (M+H+).

Workup

  1. filtrationThe resulting precipitate was filtered off with suction
  2. customThe product with a molecular weight of 462.54 (C10H22O12S4) was obtained in this way

Sources & evidence

ORD record
ord-6887cf9d43db422c83f65db12bd88ea4
Source dataset
uspto-grants-2010_11
Patent number
US07838528B2

Reaction notes

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