1,1'-Carbonyldiimidazole → HCID 73045997, compound

HRID 1174698Notes

Reaction equation

HRID 1174698 reaction equation
[CH3:1][N:2]1[CH2:6][CH2:5][CH:4]2[CH2:7][N:8]([C:10]3[CH:15]=[CH:14][C:13]([NH2:16])=[CH:12][CH:11]=3)[CH2:9][CH:3]12.[C:17]([N:24]1[CH:28]=[CH:27]N=[CH:25]1)(N1C=CN=C1)=[O:18].[Cl:29][C:30]1[CH:35]=[CH:34][C:33]([CH:36]2CCNC[CH2:37]2)=[CH:32][CH:31]=1>>[CH3:1][N:2]1[CH2:6][CH2:5][CH:4]2[CH2:7][N:8]([C:10]3[CH:15]=[CH:14][C:13]([NH:16][C:17]([N:24]4[CH2:25][CH2:37][CH:36]([C:33]5[CH:34]=[CH:35][C:30]([Cl:29])=[CH:31][CH:32]=5)[CH2:27][CH2:28]4)=[O:18])=[CH:12][CH:11]=3)[CH2:9][CH:3]12

Participants

4

Reactant 3

HCID 682631,1'-CarbonyldiimidazoleHCID 12036134-(4-Chlorophenyl)piperidineHCID 68427139HCID 68427139, compound

Product 1

HCID 73045997HCID 73045997, compound

Procedure

4-(1-Methylhexahydropyrrolo[3,4-b]pyrrol-5-yl)phenylamine was reacted by method A initially with carbonyldiimidazole and then with 4-(4-chlorophenyl)piperidine. The product with the molecular weight of 439.01 (C25H31ClN4O); MS (ESI): 439 (M+H+) was obtained in this way.

Workup

  1. customMS (ESI): 439 (M+H+) was obtained in this way

Sources & evidence

ORD record
ord-3a1d3c3d1bdc4b45ad07277dfcb22d33
Source dataset
uspto-grants-2010_11
Patent number
US07838547B2

Reaction notes

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