1,1'-Carbonyldiimidazole → HCID 73004887, compound

HRID 1174703Notes

Reaction equation

HRID 1174703 reaction equation
[CH3:1][N:2]1[CH:9]2[CH:5]([N:6]([C:10]3[CH:15]=[CH:14][C:13]([NH2:16])=[CH:12][CH:11]=3)[CH2:7][CH2:8]2)[CH2:4][CH2:3]1.[C:17]([N:24]1[CH:28]=[CH:27]N=[CH:25]1)(N1C=CN=C1)=[O:18].[Cl:29][C:30]1[CH:35]=[CH:34][C:33]([CH:36]2CCNC[CH2:37]2)=[CH:32][CH:31]=1>>[CH3:1][N:2]1[CH:9]2[CH:5]([N:6]([C:10]3[CH:15]=[CH:14][C:13]([NH:16][C:17]([N:24]4[CH2:25][CH2:37][CH:36]([C:33]5[CH:34]=[CH:35][C:30]([Cl:29])=[CH:31][CH:32]=5)[CH2:27][CH2:28]4)=[O:18])=[CH:12][CH:11]=3)[CH2:7][CH2:8]2)[CH2:4][CH2:3]1

Participants

4

Reactant 3

HCID 682631,1'-CarbonyldiimidazoleHCID 12036134-(4-Chlorophenyl)piperidineHCID 68427809HCID 68427809, compound

Product 1

HCID 73004887HCID 73004887, compound

Procedure

4-(4-Methylhexahydropyrrolo[3,2-b]pyrrol-1-yl)phenylamine was reacted by method A with carbonyldiimidazole and finally with 4-(4-chlorophenyl)-piperidine. The product with the molecular weight of 439.01 (C25H31ClN4O); MS (ESI): 439 (M+H+) was obtained in this way.

Workup

  1. customMS (ESI): 439 (M+H+) was obtained in this way

Sources & evidence

ORD record
ord-2f145ffb4a6a4492917693af78627b3f
Source dataset
uspto-grants-2010_11
Patent number
US07838547B2

Reaction notes

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