HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Fluoroindole-2-carboxylic acid → HCID 76601345, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Fluoroindole-2-carboxylic acid | HCID 1820 | — |
| Reactant | 2-(3-Dimethylamino-pyrrolidin-1-yl)-benzothiazol-6-ylamine | HCID 63231507 | — |
| Product | HCID 76601345 | HCID 76601345 | 28% |
Reaction Steps
Prepare according to Method B, using 5-fluoroindole-2-carboxylic acid (110 mg, 0.614 mmol) and 2-(3-dimethylamino-pyrrolidin-1-yl)-benzothiazol-6-ylamine (162 mg, 0.618 mmol) to yield the title compound (45 mg, 28%). mass spectrum (m/e): 424 [M+H], 422 [M−H].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07838543B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-4eb3e4bcaf8640009a7ceba5fde064a2 |
| Source note | uspto-grants-2010_11 |