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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1174955Generated: November 2, 2026

HCID 57771688, compound → HCID 57771791, compound

https://huagongshe.com/reaction/1174955

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 57771688HCID 57771688—
CatalystIronHCID 23925—
SolventAcetic AcidHCID 176—
ProductHCID 57771791HCID 57771791—

Reaction Steps

The title compound is prepared according to the procedure outlined in Example 61, Step 3 using methyl(5-nitro-benzooxazol-2-yl)-(2-pyrrolidin-1-yl-ethyl)-amine (160 mg, 0.55 mmol), iron powder (154 mg, 2.75 mmol), and acetic acid (5 mL) to yield 60 mg (42%) of product: mass spectrum (ion-spray): (m/z)=261.2 (M+1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07838543B2
Source datasetuspto-grants-2010_11
ORD IDord-88178dd9240a42f8bad24e7ceba225a5
Source noteuspto-grants-2010_11