HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dichlorobenzeneboronic acid → HCID 11533385, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dichlorobenzeneboronic acid | HCID 2734661 | — |
| Reactant | HCID 68773528 | HCID 68773528 | — |
| Product | HCID 11533385 | HCID 11533385 | — |
Reaction Steps
The title compound is prepared by following a procedure analogous to Example 113, Step 1, using N-{2-[(2-dimethylamino-ethyl)-methyl-amino]-benzothiazol-yl}-4-iodo-benzamide (0.15 g, 0.31 mmol) and 2,3-dichloro-phenyl boronic acid (0.072 g, 0.38 mmol) to afford 0.13 g (83%). LC/MS, Retention time=5.08 min; (m/z): calcd for C25H24Cl2N4OS: 499.5; found: 499.0.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07838543B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-0f483ae3bbaa42d293b3a357905fe7e9 |
| Source note | uspto-grants-2010_11 |