3-Tolylboronic acid → HCID 57771754, compound

Participants

Reaction Steps

The title compound is prepared by following a procedure analogous to Example 113, Step 1, using N-{2-[(2-dimethylamino-ethyl)-methyl-amino]-benzothiazol-6-yl}-4-iodo-benzamide (0.10 g, 0.21 mmol) and 3-methyl-phenyl boronic acid (0.037 g, 0.27 mmol) to afford 0.048 g (51%). LC/MS, Retention time=4.96 min; (m/z): calcd for C2H26N4OS (M+H)+: 445.6; found: 445.0.

Provenance & Evidence