2,5-Dichlorobenzeneboronic acid → HCID 57771761, compound

Participants

Reaction Steps

The title compound is prepared by following a procedure analogous to Example 113, Step 1, using N-{2-[(2-dimethylamino-ethyl)-methyl-amino]-benzothiazol-6-yl}-4-iodo-benzamide (0.12 g, 0.25 mmol) and 2,5-dichloro-phenyl boronic acid (0.057 g, 0.30 mmol) to afford 0.098 g, (79%). LC/MS, Retention time=5.29 min; (m/z): calcd for C25H24Cl2N4OS: 499.5; found: 499.0.

Provenance & Evidence