HCID 11659901, compound → HCID 11630799, compound

Participants

Reaction Steps

11.77 g of 4-(2-ethoxy-2-oxoethyl)-1,1-dimethylpiperazinium iodide (22) was refluxed in 600 ml water for 48 h. The reaction mixture was evaporated to dryness and the product was crystallized with diethyl ether from ethanol. Yielded white powder 5.484 g (51%). 1H NMR at 300K (D2O): δ 3.30 (6H, s), 3.51 (4H, s), 3.69 (2H, s), 3.73 (4H, bm)

Provenance & Evidence