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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1175218Generated: November 2, 2026

Methanol → HCID 68689367, compound

https://huagongshe.com/reaction/1175218

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantSodium HydroxideHCID 14798—
ReactantHCID 90254651HCID 90254651—
SolventTetrahydrofuranHCID 8028—
ProductHCID 68689367HCID 68689367—

Reaction Steps

To a solution of the title compound of Step 3 (62.7 mg, 0.175) in 1.00 ml of THF was added 1.00 ml of 6 N NaOH and 1.00 ml MeOH. The resulting mixture was stirred overnight. The mixture was acidified to neutral pH, concentrated and the title compound was purified on a Biotage MPLC.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07838676B2
Source datasetuspto-grants-2010_11
ORD IDord-a8185ddd0b8d4ca6984ab32d5cdd4f4f
Source noteuspto-grants-2010_11