HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 68689367, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 90254651 | HCID 90254651 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 68689367 | HCID 68689367 | — |
Reaction Steps
To a solution of the title compound of Step 3 (62.7 mg, 0.175) in 1.00 ml of THF was added 1.00 ml of 6 N NaOH and 1.00 ml MeOH. The resulting mixture was stirred overnight. The mixture was acidified to neutral pH, concentrated and the title compound was purified on a Biotage MPLC.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07838676B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-a8185ddd0b8d4ca6984ab32d5cdd4f4f |
| Source note | uspto-grants-2010_11 |